ORIGINAL_ARTICLE
Sol-Gel to Prepare Nickel Doped TiO2 Nanoparticles for Photocatalytic Treatment of E 131 VF Food Dye Wastewater
Sol–gel method was applied for synthesis of TiO2 nanoparticles in the existence of different volumes of ethanol (10–50 mL) with the purpose to find optimized synthesis conditions. Also, nickel doped TiO2 nanoparticles (Ni/TiO2 molar ratio: 0.1-1.0%) were prepared by the similar technique but in the existence of 10 mL ethanol and heated at different temperatures (300 °C –600 °C). XRD, SEM/EDX, UV-Vis DRS, FTIR and Raman spectroscopy were applied to identify the structural and morphological characteristics of the as-synthesized samples. XR diffraction results verified that TiO2 samples prepared with various volumes of ethanol (10–50 mL) consist of anatase and brookite phases up to 500 °C and rutile phase at 600 °C. The intensity of brookite diffraction decreased with the increase of calcination temperatures. Also, the low ethanol volume favored for formation of rutile phase at 600 °C. The addition of Ni(II) during the preparation of TiO2 nanoparticles prevented the formation of rutile phase. The undoped samples were synthesized with 10 and 20 mL ethanol and treated at 500 °C displayed the best catalytic performance for photocatalytic treatment of E 131 VF dye solution (rate constant: 0.051 and 0.061 (a.u) respectively). Ni doped TiO2 samples displayed lower photoactivity and rate constant.
https://www.jwent.net/article_244576_05c5a687aae9d22a7d2a83af70769256.pdf
2021-04-01
92
108
10.22090/jwent.2021.02.001
Sol-gel
Ni/TiO2
Ethanol
Food dye E 131 VF
Kinetic study
Malak
Barakat
malak17_barakat@hotmail.com
1
Inorganic and Organometallic Coordination Chemistry Laboratory (LCIO), Faculty of Sciences (I), Lebanese University, Rafic Hariri Campus, El Hadath, Lebanon
AUTHOR
Rassil
Khoder
khoderrassil@gmail.com
2
Inorganic and Organometallic Coordination Chemistry Laboratory (LCIO), Faculty of Sciences (I), Lebanese University, Rafic Hariri Campus, El Hadath, Lebanon
AUTHOR
Fatima
Kassir
kassir_f@icloud.com
3
Inorganic and Organometallic Coordination Chemistry Laboratory (LCIO), Faculty of Sciences (I), Lebanese University, Rafic Hariri Campus, El Hadath, Lebanon
AUTHOR
Zeinab
Harajli
zh50@aub.edu.lb
4
Inorganic and Organometallic Coordination Chemistry Laboratory (LCIO), Faculty of Sciences (I), Lebanese University, Rafic Hariri Campus, El Hadath, Lebanon
AUTHOR
Mouhiaddine Mohamed
El Jamal
mjamal@ul.edu.lb
5
Inorganic and Organometallic Coordination Chemistry Laboratory (LCIO), Faculty of Sciences (I), Lebanese University, Rafic Hariri Campus, El Hadath, Lebanon
LEAD_AUTHOR
Azadeh
Ebrahimian Pirbazari
aebrahimian@ut.ac.ir
6
Fouman Faculty of Engineering, College of Engineering, University of Tehran
LEAD_AUTHOR
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52
ORIGINAL_ARTICLE
Efficient Pb (II) removal from wastewater by TEG coated Fe3O4 ferrofluid
Tri-ethylene glycol (TEG) coated Fe3O4 nanoparticles ferrofluid were used for Pb (II) removal from simulated wastewater. The samples were synthesized using a modified co-precipitation method. The prepared samples were characterized by different techniques including X-ray diffraction, Rietveld method, FTIR, FESEM, TEM, VSM, TGA, BET and atomic adsorption experiments. The crystallinity of nanoparticles with a cubic spinel ferrite structure and absence of impurity phases were verified using X-ray diffraction and Rietveld method. The presence of TEG was approved by FTIR and thermogravimetric analysis. The VSM results showed that the bonding between the TEG molecules and ferrite nanoparticles, reduces the surface spin disorder, influences the morphology and magnetization, and consequently increases the Pb (II) removal efficiency to a high value of 97%. The obtained high value of adsorption capacity of q=363.4 mg.g-1 with R= 91 % and q=129.4 mg.g-1 with R=97 %shows effective role of TEG coating on Pb (II) adsorption. The interesting results of this study imply that the TEG coated ferrofluid sample is suitable candidate for practical applications.
https://www.jwent.net/article_244577_ffad282dee0f11d572577f06a9cc09b7.pdf
2021-04-01
109
120
10.22090/jwent.2021.02.002
TEG-Fe3O4
Coating
Magnetization
Pb(II)
Adsorption
Sajjad
Lotfi
sajjadlotfi7306@gmail.com
1
Faculty of Physics, University of Tabriz, Tabriz, Iran
AUTHOR
Bagher
Aslibeiki
b.aslibeiki@tabrizu.ac.ir
2
Faculty of Physics, University of Tabriz, Tabriz, Iran
LEAD_AUTHOR
Mahmoud
Zarei
zarei90211@yahoo.com
3
Department of Applied Chemistry, University of Tabriz, Tabriz, Iran
AUTHOR
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34
ORIGINAL_ARTICLE
Polyether Sulfone-Graphene Oxide- Polyvinyl Pyrrolidone Nanocomposite Adsorptive Membrane for Arsenic Removal from Wastewater
Arsenic contamination poses a major public health concern and harms the environment with its toxicity. Long term exposure to a high concentration of arsenic is harmful to human health as well as the environmental biodiversity. This study is aimed to fabricate and investigate the possibility of polyethersulfone-graphene oxide-polyvinyl pyrrolidone (PES-GO-PVP) nanocomposite adsorptive membrane and use it to enhance the removal of arsenic from wastewater. The nanocomposite membrane in this study was fabricated via the non-solvent induced phase separation (NIPS) method with the addition of polyvinylpyrrolidone (PVP) as a pore-forming agent. Based on the characterization results of GO through Fourier-Transform Infrared Spectroscopy (FTIR), X-ray diffraction (XRD) and Raman spectroscopy, the existence of high quantity of oxygen based functional groups with high degree of oxidation was observed, which indicated that the GO were well-synthesized. The characterization of the membrane indicated that the addition of GO and PVP could impact the membrane hydrophilicity and mechanical stability. Three adsorption parameters (initial concentration of arsenic, pH and contact time) were then optimized using a face-centred central composite design (FCCCD). The arsenic removal efficiency of 88.6 % was obtained with 55 mg/L of initial arsenic concentration, at pH 8 and 75 minutes of contact time between PES-GO-PVP membrane and the arsenic ion. The Langmuir isotherm model fitted the equilibrium data, describing the monolayer adsorption mechanism occurred on the surface of the membrane. Therefore, the results obtained in this study prove the suitability and promising potential of the nanocomposite membrane for effective removal of arsenic through adsorption.
https://www.jwent.net/article_244578_f31d07c52425cfe17211136780450cba.pdf
2021-04-01
121
137
10.22090/jwent.2021.02.003
Graphene oxide-based membrane
Characterization
Adsorption
Optimization
Adsorption isotherm
Nik Rashida
Nik Abdul Ghani
nikrashida@iium.edu.my
1
Department of Biotechnology Engineering, Kulliyyah of Engineering, International Islamic University. Malaysia (IIUM), Jalan Gombak, 53100 Selangor, Malaysia.
AUTHOR
Siti Syakirah
Sulaiman
sysyakirah@gmail.com
2
Department of Biotechnology Engineering, Kulliyyah of Engineering, International Islamic University. Malaysia (IIUM), Jalan Gombak, 53100 Selangor, Malaysia.
AUTHOR
Amina
Tahreen
aminatahreen@gmail.com
3
Department of Biotechnology Engineering, Kulliyyah of Engineering, International Islamic University. Malaysia (IIUM), Jalan Gombak, 53100 Selangor, Malaysia.
AUTHOR
Mohammed Saedi
Jami
saedi@iium.edu.my
4
Department of Biotechnology Engineering, Kulliyyah of Engineering, International Islamic University. Malaysia (IIUM), Jalan Gombak, 53100 Selangor, Malaysia.
LEAD_AUTHOR
1. Shaji E, Santosh M, Sarath KV, Prakash P, Deepchand V, Divya BV. Arsenic contamination of groundwater: A global synopsis with focus on the Indian Peninsula. Geoscience Frontiers. 2021;12(3):101079.
1
2. Karnib M, Kabbani A, Holail H, Olama Z. Heavy Metals Removal Using Activated Carbon, Silica and Silica Activated Carbon Composite. Energy Procedia. 2014;50:113-20.
2
3. Mukhopadhyay M, Lakhotia SR, Ghosh AK, Bindal RC. Removal of arsenic from aqueous media using zeolite/chitosan nanocomposite membrane. Separation Science and Technology. 2018;54(2):282-8.
3
4. Ungureanu G, Santos S, Boaventura R, Botelho C. Arsenic and antimony in water and wastewater: Overview of removal techniques with special reference to latest advances in adsorption. Journal of Environmental Management. 2015;151:326-42.
4
5. Hussain MM, Wang J, Bibi I, Shahid M, Niazi NK, Iqbal J, et al. Arsenic speciation and biotransformation pathways in the aquatic ecosystem: The significance of algae. Journal of Hazardous Materials. 2021;403:124027.
5
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57
ORIGINAL_ARTICLE
Highly active Fe-doped ZIF-8 nanocatalyst in electrochemical degradation of pharmaceutical pollutant in neutral environment
In this study, zeolitic imidazolate framework (ZIF-8) nanocatalyst was synthesized by the thermal solvent method and doped by Fe species through wet impregnation technique. The nanocatalysts were applied for the degradation of Phenazopyridine Hydrochloride (PHP) through the heterogeneous Electro-Fenton (HEF) process. The nanocatalysts were characterized by XRD, BET-BJH, FT-IR, FE-SEM, TEM, and acidimetric-alkalimetric titration techniques. The results showed the high surface area (1335 m2g-1) and homogenous dispersion of Fe species. The influence of different operating conditions was investigated, including pH level, nanocatalyst concentration, applied current, and PHP concentration. The optimum conditions for the HEF system over the Fe-ZIF-8 nanocatalyst were pH=7, 0.2 g L-1 of the Fe-ZIF-8 nanocatalyst, 100 mA, and 10 ppm of PHP concentration, which resulted in 99% PHP removal. The developed nanocatalyst had high reusability for the PHP removal in the HEF process. The results confirm the high potential of ZIF-8 nanocatalyst for pharmaceutical wastewater treatment through the HEF process.
https://www.jwent.net/article_244579_ebf9590adeddc0f12764570ee2a265e0.pdf
2021-04-01
138
149
10.22090/jwent.2021.02.004
Water treatment
Electro-Fenton
nanocatalyst
Metal-organic framework
ZIF-8
shima
Amani
m_rostamizadeh@yahoo.com
1
Department of Chemical Engineering, Sahand University of Technology, Tabriz, Iran
AUTHOR
Mohammad
Rostamizadeh
rostamizadeh.m@gmail.com
2
Department of Chemical Engineering, Sahand University of Technology, Tabriz, Iran
LEAD_AUTHOR
Ali
Ghadimi
chemeng.proj@gmail.com
3
Faculty of Petrochemicals, Iran Polymer and Petrochemical Institute, Tehran, Iran
AUTHOR
1. Adel Niaei H, Rostamizadeh M. Adsorption of metformin from an aqueous solution by Fe-ZSM-5 nano-adsorbent: Isotherm, kinetic and thermodynamic studies. The Journal of Chemical Thermodynamics. 2020;142:106003.
1
2. Lin C-C, Lee C-Y. Adsorption of ciprofloxacin in water using Fe3O4 nanoparticles formed at low temperature and high reactant concentrations in a rotating packed bed with co-precipitation. Materials Chemistry and Physics. 2020;240:122049.
2
3. Abbasi AR, Hatami S. Comparison of Structure of Nano Zinc Metal–Organic Frameworks Upon Uptake and Release of Phenazopyridine Hydrochloride. Journal of Inorganic and Organometallic Polymers and Materials. 2017;27(6):1941-9.
3
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4
5. Tian J, Sharshar MM, Yang M, Mu T, Xing J. Degradation of Rhodamine B at neutral pH using modified sponge iron as a heterogeneous electro-Fenton catalyst. Environmental Progress & Sustainable Energy. 2017;37(3):989-95.
5
6. Saini R, Kumar Mondal M, Kumar P. Fenton oxidation of pesticide methyl parathion in aqueous solution: kinetic study of the degradation. Environmental Progress & Sustainable Energy. 2016;36(2):420-7.
6
7. Rostamizadeh M, Jafarizad A, Gharibian S. High efficient decolorization of Reactive Red 120 azo dye over reusable Fe-ZSM-5 nanocatalyst in electro-Fenton reaction. Separation and Purification Technology. 2018;192:340-7.
7
8. Dolatabadi M, Ahmadzadeh S, Ghaneian MT. Mineralization of mefenamic acid from hospital wastewater using electro‐Fenton degradation: Optimization and identification of removal mechanism issues. Environmental Progress & Sustainable Energy. 2019;39(3).
8
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9
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10
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15. Andrew Lin K-Y, Hsieh Y-T. Copper-based metal organic framework (MOF), HKUST-1, as an efficient adsorbent to remove p-nitrophenol from water. Journal of the Taiwan Institute of Chemical Engineers. 2015;50:223-8.
15
16. Haque E, Lee JE, Jang IT, Hwang YK, Chang J-S, Jegal J, et al. Adsorptive removal of methyl orange from aqueous solution with metal-organic frameworks, porous chromium-benzenedicarboxylates. Journal of Hazardous Materials. 2010;181(1-3):535-42.
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17
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18
19. Thi Thanh M, Vinh Thien T, Thi Thanh Chau V, Dinh Du P, Phi Hung N, Quang Khieu D. Synthesis of Iron Doped Zeolite Imidazolate Framework-8 and Its Remazol Deep Black RGB Dye Adsorption Ability. Journal of Chemistry. 2017;2017:1-18.
19
20. Pan Y, Li Z, Zhang Z, Tong X-S, Li H, Jia C-Z, et al. Adsorptive removal of phenol from aqueous solution with zeolitic imidazolate framework-67. Journal of Environmental Management. 2016;169:167-73.
20
21. Wu Y-n, Zhou M, Zhang B, Wu B, Li J, Qiao J, et al. Amino acid assisted templating synthesis of hierarchical zeolitic imidazolate framework-8 for efficient arsenate removal. Nanoscale. 2014;6(2):1105-12.
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22. Khataee A, Rad TS, Vahid B, Khorram S. Preparation of zeolite nanorods by corona discharge plasma for degradation of phenazopyridine by heterogeneous sono-Fenton-like process. Ultrasonics Sonochemistry. 2016;33:37-46.
22
23. Eskandarloo H, Badiei A, Behnajady MA, Afshar M. Enhanced photocatalytic removal of phenazopyridine by using silver-impregnated SiO2–TiO2 nanoparticles: optimization of synthesis variables. Research on Chemical Intermediates. 2015;41(12):9929-49.
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24. Abbasi AR, Karimi M, Masoomi MY. Effect of construction method and surface area for nano metal−organic framework HKUST-1 upon adsorption and removal of phenazopyridine hydrochloride. Colloids and Surfaces A: Physicochemical and Engineering Aspects. 2017;520:193-200.
24
25. Eskandarloo H, Badiei A, Behnajady MA, Ziarani GM. Ultrasonic-assisted degradation of phenazopyridine with a combination of Sm-doped ZnO nanoparticles and inorganic oxidants. Ultrasonics Sonochemistry. 2016;28:169-77.
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26
27. Md Nordin NAH, Racha SM, Matsuura T, Misdan N, Abdullah Sani NA, Ismail AF, et al. Facile modification of ZIF-8 mixed matrix membrane for CO2/CH4 separation: synthesis and preparation. RSC Advances. 2015;5(54):43110-20.
27
28. Liao Y-T, Chen JE, Isida Y, Yonezawa T, Chang W-C, Alshehri SM, et al. Cover Picture: De Novo Synthesis of Gold-Nanoparticle-Embedded, Nitrogen-Doped Nanoporous Carbon Nanoparticles (Au@NC) with Enhanced Reduction Ability (ChemCatChem 3/2016). ChemCatChem. 2016;8(3):473-.
28
29. Morabito JV, Chou L-Y, Li Z, Manna CM, Petroff CA, Kyada RJ, et al. Molecular Encapsulation beyond the Aperture Size Limit through Dissociative Linker Exchange in Metal–Organic Framework Crystals. Journal of the American Chemical Society. 2014;136(36):12540-3.
29
30. Tran UPN, Le KKA, Phan NTS. Expanding Applications of Metal−Organic Frameworks: Zeolite Imidazolate Framework ZIF-8 as an Efficient Heterogeneous Catalyst for the Knoevenagel Reaction. ACS Catalysis. 2011;1(2):120-7.
30
31. Hassani A, Soltani RDC, Karaca S, Khataee A. Preparation of montmorillonite–alginate nanobiocomposite for adsorption of a textile dye in aqueous phase: Isotherm, kinetic and experimental design approaches. Journal of Industrial and Engineering Chemistry. 2015;21:1197-207.
31
32. Sajjadi S, Khataee A, Darvishi Cheshmeh Soltani R, Bagheri N, Karimi A, Ebadi Fard Azar A. Implementation of magnetic Fe3O4@ZIF-8 nanocomposite to activate sodium percarbonate for highly effective degradation of organic compound in aqueous solution. Journal of Industrial and Engineering Chemistry. 2018;68:406-15.
32
33. Zhang X, Liu Y, Jiao Y, Gao Q, Wang P, Yang Y. Enhanced selectively removal uranyl ions from aqueous solution by Fe@ZIF-8. Microporous and Mesoporous Materials. 2019;277:52-9.
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35
36. Rakibuddin M, Kim H. Sol-gel derived Fe3O4 quantum dot decorated silica composites for effective removal of arsenic (III) from water. Materials Chemistry and Physics. 2020;240:122245.
36
37. Wang Y, Zhao H, Chai S, Wang Y, Zhao G, Li D. Electrosorption enhanced electro-Fenton process for efficient mineralization of imidacloprid based on mixed-valence iron oxide composite cathode at neutral pH. Chemical Engineering Journal. 2013;223:524-35.
37
38. Jafarizad A, Rostamizadeh M, Zarei M, Gharibian S. Mitoxantrone removal by electrochemical method: A comparison of homogenous and heterogenous catalytic reactions. Environmental Health Engineering and Management. 2017;4(4):185-93.
38
39. Nidheesh PV, Gandhimathi R, Velmathi S, Sanjini NS. Magnetite as a heterogeneous electro Fenton catalyst for the removal of Rhodamine B from aqueous solution. RSC Advances. 2014;4(11):5698.
39
40. Nidheesh PV, Gandhimathi R. Comparative Removal of Rhodamine B from Aqueous Solution by Electro-Fenton and Electro-Fenton-Like Processes. CLEAN - Soil, Air, Water. 2013;42(6):779-84.
40
[41] Rostamizadeh, M., Jalali, H., Naeimzadeh, F., and Gharibian, S. 2019. Efficient Removal of Diclofenac from Pharmaceutical Wastewater Using Impregnated Zeolite Catalyst in Heterogeneous Fenton Process. Phys. Chem. Res., 7, 37-52.
41
42. Hou B, Han H, Jia S, Zhuang H, Xu P, Wang D. Heterogeneous electro-Fenton oxidation of catechol catalyzed by nano-Fe3O4: kinetics with the Fermi’s equation. Journal of the Taiwan Institute of Chemical Engineers. 2015;56:138-47.
42
43. Gharibian S, Hazrati H, Rostamizadeh M. Continuous electrooxidation of Methylene Blue in filter press electrochemical flowcell: CFD simulation and RTD validation. Chemical Engineering and Processing - Process Intensification. 2020;150:107880.
43
44. Saeid S, Behnajady M. Photooxidative Removal of Phenazopyridine by UV/H2O2 Process in a Batch Re-circulated Annular Photoreactor: Influence of Operational Parameters. Oriental Journal of Chemistry. 2015;31(2):1211-4.
44
45. Murugananthan M, Yoshihara S, Rakuma T, Shirakashi T. Mineralization of bisphenol A (BPA) by anodic oxidation with boron-doped diamond (BDD) electrode. Journal of Hazardous Materials. 2008;154(1-3):213-20.
45
46. Gholizadeh AM, Zarei M, Ebratkhahan M, Hasanzadeh A, Vafaei F. Removal of Phenazopyridine from wastewater by merging biological and electrochemical methods via Azolla filiculoides and electro-Fenton process. Journal of Environmental Management. 2020;254:109802.
46
47. Gholizadeh AM, Zarei M, Ebratkhahan M, Hasanzadeh A. Phenazopyridine degradation by electro-Fenton process with magnetite nanoparticles-activated carbon cathode, artificial neural networks modeling. Journal of Environmental Chemical Engineering. 2021;9(1):104999.
47
48. Yousefi A, Nezamzadeh-Ejhieh A, Mirmohammadi M. SnO2-BiVO4 mixed catalyst: Characterization and kinetics study of the photodegradation of phenazopyridine. Environmental Technology & Innovation. 2021;22:101433.
48
49. Yousefi A, Nezamzadeh-Ejhieh A, Mirmohammadi M. The coupled CuO-SnO2 catalyst: Characterization and the photodegradation kinetics towards phenazopyridine. Environmental Technology & Innovation. 2021;22:101496.
49
ORIGINAL_ARTICLE
Influence of Calcination Temperature and Operational Parameters on Fe-ZSM-5 Catalyst performance in Sonocatalytic Degradation of Phenol from wastewater
Nowadays, not only the lack of water sources but also water pollution by industrial wastewater has become a major challenge. One of the pollutants of water resources, which threatens water resources, is phenol that enters the environment through wastewater from various industries such as petrochemicals, refineries, pharmaceuticals, etc. This compound, due to its toxicity, high stability and solubility in water caused many problems and it is very important to remove it from industrial wastewater. Therefore, the main purpose of this study is to remove phenol from wastewater by using catalytic oxidation. Fe-ZSM-5 catalyst was synthesized by precipitation method and its characteristics were determined by XRD, FTIR, SEM and BET analyses. The results of XRD analysis showed that the iron ions are in the MFI structure and the catalyst has a good crystallinity phase, so that it retains its MFI structure. BET analysis showed the specific surface area of the synthesized catalyst is 293g/m2. The catalytic activity of Fe-ZSM-5 was investigated in degradation of phenol and the results showed that the mentioned catalyst had the highest removal percentage (85.82%) in 90 min at pH = 4.25 and T= 70 °C. The effect of various parameters such as ultraviolet radiation, initial pollutant concentration, catalyst loading and H2O2 concentration on the catalytic activity were also investigated.
https://www.jwent.net/article_244580_4296830e47ab6337697705f14e232ee7.pdf
2021-04-01
150
163
10.22090/jwent.2021.02.005
Catalytic oxidation
Fe-ZSM-5
Phenol
Wastewater treatment
Ultrasound Waves
Hamid
Kazemi Hakki
ha_kazemi@sut.ac.ir
1
Chemical Engineering Faculty, Sahand University of Technology, P.O.Box 51335-1996, Sahand New Town, Tabriz, Iran.
LEAD_AUTHOR
Pouya
Shekari
shekaripouya18@yahoo.com
2
Chemical Engineering Faculty, Sahand University of Technology, P.O.Box 51335-1996, Sahand New Town, Tabriz, Iran.
AUTHOR
Ahmad
Najafidoust
ahmad.najafidoust@gmail.com
3
Chemical Engineering Faculty, Sahand University of Technology, P.O.Box 51335-1996, Sahand New Town, Tabriz, Iran.
AUTHOR
Nosrat
Dezhvan
farhad_urmia2011@yahoo.com
4
The University of Applied Sciences and Technology Shirin Asal Branch, Tabriz, Iran
AUTHOR
Masoume
Seddighi Rad
pajooheshrad@gmail.com
5
Faculty of Science, Azad University Nnorth Tehran Branch, Tehran, Iran
AUTHOR
1. Albukhari SM, Ismail M, Akhtar K, Danish EY. Catalytic reduction of nitrophenols and dyes using silver nanoparticles @ cellulose polymer paper for the resolution of waste water treatment challenges. Colloids and Surfaces A: Physicochemical and Engineering Aspects. 2019;577:548-61.
1
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39
ORIGINAL_ARTICLE
Synthesis, Characterization and Photocatalytic study of FeCr2O4@ZnO@MgO Core-Shell Nanoparticle.
In the present work, the sol-gel derived powders of the chemical form FeCr2O4@ZnO@MgO Core-shell, has been synthesized and used as a photocatalyst. The synthesized core-shell nanoparticles characterized by various analytical techniques including FTIR, XRD, SEM-EDAX, and HR-TEM-SEAD. The successful performance of synthesized core-shell photocatalyst FeCr2O4@ZnO@MgO has been also demonstrated for the complete mineralization of Orange G dye. The effect of various operational parameters used in dye degradation such as concentration of dye, light intensity, amount of photocatalyst, effect of light and effect of electrolyte has been studied on the rate of reaction. TEM analysis clearly shows two layers of ZnO and MgO on FeCr2O4. The highest degradation rate was found with concentration of Orange G dye 10 ppm, 0.8 g of FeCr2O4@ZnO@MgO and time 50 min. The recyclability of the photocatalyst, FeCr2O4@ZnO@MgO was performed up to four runs. The degradation mechanism has been established by using LC-MS analysis and it was used to track the numerous intermediate products formed during the course of Orange G dye degradation.
https://www.jwent.net/article_244581_8b0b62d37a02610460e51697c01b1b1e.pdf
2021-04-01
164
176
10.22090/jwent.2021.02.006
Sol-gel
Photocatalytic degradation
Orange G dye
LC-MS
Ashok
Borhade
ashokborhade2007@yahoo.co.in
1
Research Centre, Department of Chemistry, HPT Arts and RYK Science College, Nashik 422005, Maharashtra, India. Affiliated to Savitribai Phule Pune University, Pune-411007, Maharashtra, India
LEAD_AUTHOR
Dipak
Tope
dipak.tope@gmail.com
2
Research Centre, Department of Chemistry, HPT Arts and RYK Science College, Nashik 422005, Maharashtra, India. Affiliated to Savitribai Phule Pune University, Pune-411007, Maharashtra, India
AUTHOR
Jyoti
Agashe
jyotiagashe@gmail.com
3
Research Centre, Department of Chemistry, HPT Arts and RYK Science College, Nashik 422005, Maharashtra, India. Affiliated to Savitribai Phule Pune University, Pune-411007, Maharashtra, India
AUTHOR
Sachin
Kushare
sachinkushare7@gmail.com
4
Research Centre, Department of Chemistry, HPT Arts and RYK Science College, Nashik 422005, Maharashtra, India. Affiliated to Savitribai Phule Pune University, Pune-411007, Maharashtra, India
AUTHOR
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41
ORIGINAL_ARTICLE
Investigation on the photocatalytic activity of chemically synthesized zirconium doped cadmium selenide nanoparticles for indigo carmine dye degradation under solar light irradiation
A simple chemical methodology has been adopted for the synthesis of zirconium (Zr) doped and un-doped cadmium selenide (CdSe) nanoparticles for the application towards photocatalytic degradation of indigo carmine (IC) dye under solar light irradiation. The as prepared Zr-CdSe (doped) and CdSe (un-doped) nanoparticles were characterized by ultraviolet visible spectroscopy (UV-vis), X-ray diffraction (XRD), Scanning electron microscopy (SEM) coupled with energy dispersive X-ray analysis (EDAX) and Transmission electron microscopy (TEM) studies. The inclusion of Zr ion into the CdSe nanoparticles matrix was confirmed by SEM-EDAX and XRD studies. TEM studies confirm the zirconium ions are uniformly doped over the CdSe surface. The photocatalytic degradation performance of Zr doped and un-doped CdSe nanoparticles were examined for the degradation of IC dye under solar light irradiation. The experimental results showed that the Zr doped CdSe possessed greater photocatalytic activity in comparison to un-doped CdSe. Photodegradation process parameters such as the initial concentration of the dye, as well as the amount of catalyst and time were investigated. The photocatalytic degradation rate was favored by a high concentration of solution in respect to Langmuir–Hinshelwood model.
https://www.jwent.net/article_244582_c207a51144253628b3af2b9b0cf2cb88.pdf
2021-04-01
177
187
10.22090/jwent.2021.02.07
Zr doped CdSe nanoparticles
indigo carmine dye
solar irradiation
Photocatalysis
Emelda
Rayappan
1
Department of Chemistry, Annai Velankanni College (Affiliated to Manonmaniam Sundaranar University, Tirunelveli – 627012), Tholayavattam-629157, TN, India
AUTHOR
Jayarajan
Muthaian
2
Department of Chemistry, Annai Velankanni College (Affiliated to Manonmaniam Sundaranar University, Tirunelveli – 627012), Tholayavattam-629157, TN, India
AUTHOR
Muthirulan
Pandi
pmuthirulan@gmail.com
3
Department of Chemistry, Lekshmipuram College of Arts and Science (Affiliated to Manonmaniam Sundaranar University, Tirunelveli – 627012), Neyyoor-629802, TN, India
LEAD_AUTHOR
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ORIGINAL_ARTICLE
Nano Fe-oxide and nano-hydroxyapatite can decrease the Cd uptake by plant in a soil treated with Cd-polluted sewage sludge
Decreasing the heavy metals availability has important key factors in environmental studies. This research was done to investigate the effect of nano-Fe oxide and nano-hydroxyapatite (NHAP) on Cd uptake by plant that cultivated in the sewage sludge amended soil. Treatments consisted of applying Cd (0, 10 and 20 mg Cd/kg)-polluted sewage sludge at the rates of 0, 15 and 30 t/ha, nano-Fe oxide (0 and 0.5 ppm) and NHAP (0, 0.5 and 1 % (W/W)). The plant in this experiment was pinto bean (Cv. Khomein). After 90 days, the plants were harvested and the plant Zn, Cd and Fe concentration was measured using AAS. In addition, soil microbial respiration was calculated. Soil application of NHAP significantly increased the Zn and Fe concentration of the plants that cultivated in the soil which was amended with 15 t/ha sewage sludge by 12.8 and 14.5%, respectively. However, the Cd concentration was decreased by 17.2%. Using 15 and 30 t/ha sewage sludge significantly increased the plant Zn and Fe by 13.1 and 14.6%, respectively. Foliar application of nano-Fe oxide ate the rate of 1 ppm significantly decreased the plant Cd uptake by 18.3%. Using NHAP (0.5 % (W/W)) and sewage sludge (30 t/h) significantly increased the soil microbial respiration by 14.2 and 15.3%, respectively. The results of this study showed that using organic amendments such as NHAP and sewage sludge or foliar application of nano-Fe oxide can affect in decreasing the heavy metal uptake by plants that is a positive point in environmental studies.
https://www.jwent.net/article_244583_e97f68f175992d16d261dbc1b25cf2c9.pdf
2021-04-01
188
195
10.22090/jwent.2021.02.008
Sewage sludge
CD
NHAP
Remediation
Nano-Fe oxide
Amir Hossein
Baghaie
a-baghaie@iau-arak.ac.ir
1
Department of Soil Science, Arak Branch, Islamic Azad University, Arak, Iran
LEAD_AUTHOR
Aminollah
Aghilizefreei
amin@yahoo.com
2
Department of Chemical Engineering, Isfahan University of Technology, Isfahan, Iran
AUTHOR
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